Iranian Journal of Materials Science and Engineering
Iran University of Science & Technology
Thu, Nov 14, 2024
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Volume 11, Issue 2 (June 2014)
IJMSE 2014, 11(2): 71-78 |
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Sh. Damghanian, H. Omidvar, S. H. Tabaian, A. R. Azadmehr. FABRICATION OF A “CONE PAA NANOSTRUCTURE” BY GRADUAL DECREASE OF VOLTAGE . IJMSE 2014; 11 (2) :71-78
URL: http://ijmse.iust.ac.ir/article-1-657-en.html
URL: http://ijmse.iust.ac.ir/article-1-657-en.html
Abstract: (20212 Views)
The conical nanostructure improves the applications of alumina membranes and provides three dimensional
nanometer scale systems to study the chemical and physical properties. In this study, the nano cone structure is
produced in porous anodic alumina (PAA) by two-step anodizing. This conical nanostructure will improve the
application of PAA membranes. This approach is novel generation of the so-called "gradually decreased voltage"
technique, in which the voltage- time curve is divided into three stages and the effect of each step is investigated for
different electrolytes. The effect of the decreasing voltage is examined in two types of electrolytes oxalic and
phosphoric acid with a constant decrease in voltage rate. The results of SEM, FE-SEM images show the slope of the
inner cone layer in the oxalic acid to be considerably larger compared with phosphoric acid.
Keywords: Porous anodic alumina, anodizing, phosphoric acid, oxalic acid, nanostructures, cone porous
Type of Study: Research Paper |
Subject:
materials engineeing and special subjects
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